By Michio Inagaki Ph.D., Feiyu Kang Ph.D.
Materials technological know-how and Engineering of Carbon: Characterization discusses 12 characterization suggestions, concentrating on their program to carbon fabrics, together with X-ray diffraction, X-ray small-angle scattering, transmission electron microscopy, Raman spectroscopy, scanning electron microscopy, picture research, X-ray photoelectron spectroscopy, magnetoresistance, electrochemical functionality, pore constitution research, thermal analyses, and quantification of practical groups.
Each contributor within the publication has labored on carbon fabrics for a few years, and their historical past and adventure will supply advice at the improvement and study of carbon fabrics and their extra applications.
- Focuses on characterization ideas for carbon fabrics
- Authored through specialists who're thought of experts of their respective techniques
- Presents useful effects on quite a few carbon fabrics, together with fault effects, so that it will aid readers comprehend the optimal stipulations for the characterization of carbon materials
Read or Download Materials Science and Engineering of Carbon. Characterization PDF
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Extra info for Materials Science and Engineering of Carbon. Characterization
Sample text
11A. 7 nm, respectively. 11 SAXS patterns for MCF-carbons and MCF-silica template (A) and the DDFs for MCF-carbons C1 and C2 (B) [17]. Reprinted with permission from Oda Y, Fukuyama K, Nishikawa K, Namba S, Yoshitake H, Tatsumi T. Mesocellular foam carbons: aggregates of hollow carbon spheres with open and closed wall structures. Chem Mater 2004;16:3860e6. Copyright © 2004 American Chemical Society. 44 nmÀ1 [16]. 6 nm. 298 nmÀ1, corresponding to a d-spacing of 21 nm, which agrees well with the average distance of two neighboring pores, 23 nm, calculated from the transmission electron microscope photograph [17].
Measurement and analysis of small-angle X-ray scattering. Ind Eng Chem Anal Ed 1946;18:172e5. 1 Introduction ....................................................................................................... 2 Modes of Transmission Electron Microscopy ....................................................... 1 Diffracting Mode .............................................................................. 2 Imaging Modes ................................................................................
4 INDEXING THE DIFFRACTION LINE As mentioned before, three-dimensional hkl lines appear only for the samples that include appreciable amounts of graphitic structure with three-dimensional regular stacking. One example is shown in Fig. 1. In the coke heat-treated at 1200 C (Fig. 1B), 002 diffraction profile is so broad, suggesting that the sample is not yet graphitized and there is no three-dimensional regular stacking, in other words, no possibility for the appearance of hkl diffractions. The broad peak observed at 2q ¼ 43 degree is neither 100 nor 101 diffraction but has to be indexed as 10 diffraction of two-dimensional hexagonal net layers.