Elsevier’s Encyclopædia of Organic Chemistry: Series III: by F. Radt (auth.), F. Radt (eds.)

By F. Radt (auth.), F. Radt (eds.)

When, many years in the past, the e-book of Elsevier's Encyclo­ pa:dia of natural Chemistry used to be suspended, it appeared fascinating to complete-on account of its monographic character-the steroid part in response to the unique belief. One conside­ ration in favour thereof, between others, used to be that the steroid portion of Beilstein's Handbuch usually are not on hand for a few future years, in order that additionally to these utilizing Beilstein the current ebook is a precious assist in bridging the space. In view of the undiminished job during this targeted box- both vital to chemists, bio­ chemists, and the scientific global - the desire that the of entirety of this part will meet the wishes of a large circle of readers ap­ pears tobe justified. Altogether 3 extra volumes are deliberate for the complement, the 1st of which, now provided, covers the steroid Oxo-com­ kilos, the Iiterature having been consulted as much as the tip of 1946 in conformity with the former volumes of the steroid complement. the place, even though, vital additions and correc­ tions are involved, Iiterature as much as the latest date has been taken into consideration. In treating the subject material an identical prin­ ciples were as within the earlier volumes of this part. Editorship is still within the useful palms of Dr. F. RADT, who has contributed a substantial share of the problem handled during this quantity. he's assisted by means of Dr. A. GEORG and Dr. DoRA STERN.

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Fmn. ; [1X]~ 2 From 21-chloropregnan-20-one (p. 2221 s) on re~ fluxing with sodium benzoate in alcohol. - Rns. I Gives 2 I -hydroxy-LI 20 <22 >-norcholenic acid Iactone ~H (partial formula I, above) on refluxing with ethyl bromoacetate and zinc in benzene, followed by heating with glacial acetic acid containing hydrogen bromide at I35-I40° (I94I Linville; I942 Fried). ~ 1 5I=:J + CO·CH ·OH Allopregnan-21-ol-20-one c21H3402. Crystals (methanol)' m. I I 5-7°. Fmn. The acetate is obtained from allopregnan-20-one ~M~~ CO·CH ·OH (p.

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